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KMID : 1059520080520050523
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Journal of the Korean Chemical Society
2008 Volume.52 No. 5 p.523 ~ p.529
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A Simple and Efficient Grindstone Chemistry Solid-state Reaction Procedure for the Synthesis of Heterocyclic Oximes in Dry Media
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M. Gopalakrishnan
J. Thanusu
V. Kanagarajan
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Abstract
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Various diverse heterocyclic oximes of 3-alkyl-2,6-diarylpiperidins, tetrahydrothiopyrans, and tetrahydropyran-4-ones are synthesized using a mortar and pestle in dry media catalyzed by activated fly ash in excellent yields and are characterized by melting point, elemental analysis, MS, FT-IR, and 1H NMR spectroscopic data.
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KEYWORD
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Oximation, Activated Fly Ash, Grindstone Chemistry, Green Chemistry
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